Summary
Type: SPE
Application #: 302980
Catalog#: 730012 - SPE Cartridges, Chromabond, C18 ec, 3ml, PP, 200mg, 50/pk
Detection: Further analysis: the residue was dissolved in 2ml of acetonitrile, HPLC
Conditions: Compounds investigated: linoleic and linolenic acid hydroperoxides
Column conditioning: For solid extraction the column has to rinse consequently with 12 ml each of MeOH and H2O
Sample application: 20ml.
Elution: with 8 ml tetrahydrofuran
Column washing: with 2 ml of H2O
Evaporation: to dryness
Authors: Zürcher A Krottenthaler M Back W
Source: TU München Lehrstuhl für Technologie der Brauerei 1